Pengaruh Penambahan Konsentrasi Ag2S Terhadap Komposit Konduktor (Ag2S)x(Na3PO4)1-x (x = 0,1 - 0,5 )

Safei Purnama, Patricius Purwanto, Grace Tj. Sulungbudi

Abstract


Komposit konduktor (Ag2S)x(Na3PO4)1-x dibuat dengan metalurgi serbuk dengan mencampurkan serbuk Ag2S dengan Na3PO4, dikompaksi dengan tekanan 48,26.106 N/m2 dan diameter 1,5.10-2 m. Komposit konduktor (Ag2S)x(Na3PO4)1-x dilakukan pemanasan pada suhu 150 °C selama 5 jam. Penentuan struktur kristal (Ag2S)x(Na3PO4)1-x dilakukan dengan teknik difraksi sinar- x. Analisis puncak difraksi sinar-x pada komposit konduktor (Ag2S)x(Na3PO4)1-x menunjukkan struktur Ag2S dan Na3PO4. Pengukuran konduktivitas komposit konduktor (Ag2S)x(Na3PO4)1-x dilakukan dengan alat LCR-meter pada frekuensi 0,1 Hz sampai dengan 100 kHz. Konduktivitas komposit konduktor (Ag2S)x(Na3PO4)1-x naik dan impedansinya turun seiring dengan naiknya konsentrasi Ag2S. Analisis morfologi permukaan komposit konduktor (Ag2S)x(Na3PO4)1-x dilakukan dengan mikroskop elektron, hasil menunjukkan terjadi perubahan seiring dengan bertambahnya konsentrasi Ag2S. 


Keywords


Komposit, Difraksi sinar-x; Konduktivitas; Struktur mikro

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DOI: http://dx.doi.org/10.24817/jkk.v38i2.2701

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